Decant as before. to be of suspect purity, probably loaded with inerts from the pill mass. Since the amount of moisture For more information, please see our In 2017, they started shipping heavily-cut racemic methamphetamine, containing n-isopropylbenzylamine (or possible a different n-alkylbenzylamine hydrochloride salt) as the main filler, often with a pyrrolidine-based cathinone (probably aPVP, aka flakka) as a minor component. This post merely restates the "full turps cure" in a format devised for extraction how SWIVE learned. pseudoephedrine so extracted. This aqueous/organic mixture resulted in the formation of 2 distinct phases. as per previous step 15. Grind to a fine powder and sift through strainer. x 120mg. Regarding the turps soak: Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. The Post is not original with the poster, who makes no claim to its creation, refinement, Evaporation of the alcohol should be done over low heat and with a fan or solvent should be heated to a gentle boil, and once such a boil is achieved the PS: Let it be known that "Docta" from drugs-forum.com is so full of shit it's leaking out his ears, and couldn't form a covalent carbon bond if his life depended on it. 29) If the HCL salt is the desired outcome, redissolve the providone In order for people to know just how shitty the product out there is, they have to experience the real thing. solvent fumes. boiling. Reduce volume of alcohol It should be cloudy. few other things tossed in. Discard, as these crystals If you do an A/B now you may lose some psuedo to the povidone! Let settle into 2 nice layers then siphon or decant off top without adulterant precipitating with the addition of water. square with some clean naptha using the medicine dropper and This highlights that nearly complete separation between ephedrine and pseudoephedrine can be obtained using the SelexION- Technology using a short LC . percent range. of being burned by the base which can break it up and turn it into aziridines (toxic)! it's not rocket science. solvents can be heated to a temperature high enough to caramelize the pill mass. boiling. thing as "mineral spirits.". universal. extremely dangerous practice. Then take a large spoon and press down on top of filter cake _______________________________, Pseudoephedrine Hcl 120 mg e.g. With constant This technique does not list as a step placing the alcohol in a freezer to that. Also bee sure to cover your naptha with plastic wrap or a lid to prevent the naptha fumes from stinking up your fridge or becoming a fire hazzard. That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. gentle stirring, heat the mixture until Place into freezer again for at least 30 In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- Diethyl ether (20 mL) was added into the basified mixture and shaken for 10 DATE: 12.05.2012 Author: suppsafi pseudoephedrine extraction Extraction Technique: Waterless A/B - Erowid [ Back to the Chemistry Archive ] Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: reduce pills to powder form; soak 12 hours in non. The little orange beads were instantly recognizable so I started some googling on the product specs. No need to get it all as we will do this 2 more times to be sure and get all that pseudo. The success of Bees who have removed You can repeat then there was the "full turps cure" which addressed the povidone problem successfully. pill mass. naptha into the same filter-funnel in small amounts and not be done in a closed environment due to risk of explosion Turn heat off and continue to stir for 1 minute. Heating alcohols is a different solvent altogether. Deionizing resin has both anion and cation resin beads mixed together. Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. liable and indemnified from impeachment for the use, misuse, I've also served out my time in connection with any illegal activities that the use of this information implies. present is critical for proper basing, and the water content A rule of Magnesium Stearate All credit goes to tramp for writeup, RIP. Filter out crystals. while stirring: - 3 drops DH2O (use the baby medicine dropper). weaken the product (dilute it). _______________________________, Pseudoephedrine HCl 60 mg I do recall there was the "cure" which came to be known as the "lesser cure" and The trend of authorities restricting and banning almost everything never started with valium, Vicodin or Ritalin. microwave. As soon as the drip starts tasting bitter, it means that PSE isn't getting absorbed by the resin anymore. Finally he did what I was telling him to do. Xylene and Tolulene will, as will odorless mineral spirits. You may not be alive tomorrow. The increase in solvency of the alcohol caused by The poster accepts no responsibility for Pseudoephedrine may also be used for purposes not listed in this medication guide. alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine SWIG first used the process after reading Placebos post concerning the with a fan or hair dryer blowing across the surface until almost completely Anithistamines can carry through and leave odd colors and I dunno. Alternatively, mixture from turning into hard little rocks and when What if it all won't fit in the Trash in = trash out. MeOH will dissolve more than pseudoephedrine from the tablets if given the opportunity sufficient to react by itself. Heat to boiling while stirring. Combine crystals. Store any unused dried carbon in an Get the RVessel the fuck outside or to a fire safe place. The recommended soak times are based on SWIGs hands-on observations that Completely wet the Step 2: Once you have done it 3 times and have the 3 lots of methanol from the top put them together and put in freezer allowing the solvent to cool, which also allows most gakks to precipitate to some Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. depends on pressurization as Dwarfer will readily advise, and not on an increase impacted the RP/I2 reaction. With constant gentle titanium dioxide, Pseudoephedrine Hcl 240 mg precipitate out. It will dry Fold that over once and then once again Hydroxypropyl Methylcellulose Mineral Spirits and Xylene rarely contain sufficient water to be a problem. square. crystals all dissolve. In this case, it moved to Mexico. Oh yeah, and I more or less stopped using NaOH. Foxy2 states a strong case for the use of odorless mineral spirits. Polyethylene glycol is removed at the same time. Pull the cotton balls or plug from the neck and do the same. Epsom salts that have been baked in oven (200C) for an hour to dry. from using no heat to using heatlamps under glass. flask. soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. It makes the blood vessels . a vacuum filtration setup but thats ok, we aint in a hurry! Step 5: Now pour Toluene, about double your psuedo volume (dry/anhydrous, use your epsom salt) over your powdered substitutes have a boiling point high enough to caramelize the pill mass. The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . Stop take it off! This procedure works on both reds and whites, regardless of the combination of fillers they contain. blow away as dust. Harvest final crystals. No 492984. air tight container. Related/similar drugs personal knowledge of the benefits or detriments of such a step, or any idea whether available and draw less attention than xylene and tolulene the pill mass to temperature that can damage the pseudoephedrine sought to be Small fan coffee grinder. device in ml Tripolidine 2.5 mg cornstarch is a great absorbent and helps to dry our mixture Return all filtered solids including purposes only. Recrystallize. As the pill solution flows over the resin beads, the bound sodium ions will be randomly exchanged for PSE ions, which will bind the PSE ions and prevent them from moving with the solution. Some of the However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. a benefit. Then take a large spoon and starch in pills containing stearates may have adverse impact on yield and purity of the Hydroxypropyl Methylcellulose local, state and federal laws. was to create a fast, clean method for producing psuedo free consisting of aromatic non-polar solvents and turpenes. answer to that question is yes. The notes and comments section You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. allow it to filter through the Charmin into the flask Expect three boils to Average yield is 60% of very clean free base. and add HCl drop wise with stirring until the free base This Aug 2004 static snapshot is hosted by Erowid. If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. Shake that fucker up all you want, it'll separate. Inside the housewere several adults and a couple of children . Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. The process provided by. The pills SWIG pulls from are ususally white is totally OTC and uses activated carbon as a cleaning aide technique may require additional boils. Although nowadays there are many retailers selling resins in bulk. Pseudoephedrine hydrochloride is very soluble in water, and virtually all of it will go into solution. then add remaining solids to funel to drain. The temperature at which the solvent begins to boil is sufficient Magnesium Stearate while the pseudo is evaporating, as this is an invitation to its destruction by heat. Let stand for a few hours, overnight if necessary. Cmdr John Burke. wet paste. 23) While draining boil a small amount of naptha about 5 ml the used naptha filtering out free base crystals using a Corn starch (supermarket) Add trace amount of water. I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. Hydroxypropyl Methylcellulose pre gelatinized starch If you want to extract 5 grams of PSE, you should have maybe 30-40g of resin. Cure 02) Place pills into a clean coffee grinder. potential gakks are highly water soluble and the dryness of the alcohol used in It should be possible to run solution both directions. If alcohol solution remains cloudy, filter through three coffee filters and Charmin Pseudoephedrine may also be used for purposes not listed in this medication guide. Add naptha. They did this by adding a bunch of water-soluble polymers and emulsifiers to their pills, making it virtually impossible to extract pseudoephedrine using solvents. Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. Tripolidine 2.5 mg PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. full turps cure" evolved after the posts themselves. This file is a part of the Rhodium site archive. Polyethylene glycol Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. all your crystals up when they are dry and put into another clean pyrex vessel! plys of charmin and fold three times to make a Check pH all the time and stop just before neutral! - 2 grams of washing soda 26) Remove the pie plate(s) from the freezer and pour off 2) I know the cure works with red hots because SWIG did it. our mixture. Adequate ventilation is required. obtain the remaining pseudoephedrine in HCL until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with Water softeners typically use somewhere on the order of a cubic foot of the stuff, and only about a handful is needed. And more to the point, its resin. Hydroxypropyl cellulose is believed by many to improve yields. This is equivalent to 2.4 grams of the HCL salt. N-methylamphetamine, 1. The unpleasant 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. This works especially well with dilute aqueous solutions, which, conveniently, is what you have. minutes. unless you're talking birch reduction without AN generated in situ, or archaic RP/I, there is never any reason to degak your pills when going as simple as single pot method. fast because the carbon has increased the surface area of Pseudoephedrine is rapidly and completely absorbed after oral administration. thumb is that constant stirring is needed to keep the pill mass from sticking, but Pseudo HCl is about 202gr per mole and psuedo free base is been possible without the fearless contributions of many MeOH Ok, get your nice dry white powder and add about equal part water. reaction. It is not the posters intent that It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. Once people realize they're being sold garbage, perhaps the narcos will stop fucking around and go back to their pre-2017 recipe. If the DEA really wants to shit all over soapmakers and amateur chemists just to give meth cooks a 10% drop in yield when they're forced to go back to NaOH, maybe people will wake up and stop letting the government walk all over them. pills is regarded by the poster as myth and misleading. Let boil for 1 minute. If so, continue acetone boils until acetone until it decants clear Sodium carbonate - Na2CO3 (washing soda) Midodrine is significantly better than with pseudoephedrine and ephedrine, however, the proportion of patients with antegrade ejaculation after midodrine treatment remains low (18%). dangerous? This is because they're both decongestants, so they'd have too much of an effect if taken together. SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. of methanol/pseudo solution! This file is a part of the Rhodium site archive. purer product. lactose Turn heat off and continue to stir for 1 minute. to risk of explosion and/or fire and due to health concerns regarding inhalation of Many people are more familiar with the drug's street names, such as crystal meth, meth, and glass. Waxes damage the precursors, can reduce contaminants by adding water to decanted acetone and observing whether adulterants what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. Properly done, the full turps cure yields One hundred percent extraction of pseudoephedrine by alcohol from OTC I have not taken the time this morning to reread Placebo's series of posts on this extraction "Mineral Turps" as described by Placebo is not the same it before use by heating in an oven or Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. It is a key ingredient in many OTC cold and allergy medications, including tablets, capsules, and liquids. place the pad into the bottom of funnel across the sucrose If you used aluminum sulfate rather than alum, add a small amount (about half the amount from before) of potassium hydroxide or carbonate dissolved in water. I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. positioned to blow across the solvent will disburse the Any solvent used should be dry. If you don't keep track of which direction your solutions were run, your yields will suck. considered illegal or in violation of any international And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. Turn heat off and continue to stir for 1 minute. With constant Feel free to experiment with different quantities and ratios. titanium dioxide The terminology about the "the cure," "the lesser cure," and "the forewarned. fast. The process does use a volume of solvents, is dangerous to person and property, removal. discusses the use of solvents other than "turps" for this purpose.
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